Journal of Organic Chemistry p. 955 - 963 (1983)
Update date:2022-09-26
Topics:
Olah, George A.
Krishnamurthy, V. V.
Singh, Brij P.
Iyer, Pradeep S.
Thermolysis of a series of ω-arylalkanoyl m-chlorobenzoyl (and acetyl) peroxides at ca. 100 deg C in cyclohexanone and in hexachloroacetone was studied by using 13C chemically induced dynamic nuclear polarization.Analysis of the observed 13C polarizations indicate that all the three radicals (β-arylethyl, γ-arylpropyl and δ-arylbutyl) have open-chain structures with no evidence for aryl participation resulting in spirocycloalkylcyclohexadienyl radicals.
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(1981)
