Journal of Organic Chemistry p. 2644 - 2647 (1983)
Update date:2022-08-05
Topics:
Keana, John F. W.
Seyedrezai, Seyed E.
Gaughan, Glen
The synthesis of two short-chain trans-2,5-difunctionalized azethoxyl nitroxide spin-labels, dinitrile 12 and dicarboxylic acid 14, is described.The trans stereochemistry of 12 and 14 was established by conversion of 12 to a diastereomeric mixture of N-hydroxy esters 13, which was analyzed by NMR spectroscopy.
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