Chemistry of Natural Compounds p. 205 - 207 (1983)
Update date:2022-08-03
Topics:
Rabinovich, A. K.
Karelskii, V. N.
Krysin. E. P.
Antonov, A. A.
Smirnov, M. B.
Chipens, G. I.
A number of N-trityl-substituted amino acids (lysine, glutamine, tyrosine, valine, and proline) have been obtained with the aid of the silylation reaction.Bis(trimethylsilyl)acetamide was used as the silylating agent.The compounds were isolated with good yields and were distinguished by chromatographic homogeneity, and they were characterized by their angles of optical rotation, melting points, and elementary analyses.Their purity was checked by TLC and 13C NMR.
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(1987)Doi:10.1002/jhet.5570190553
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(1982)
