Tetrahedron p. 5557 - 5566 (1987)
Update date:2022-08-05
Topics: Asymmetric synthesis Column chromatography NMR spectroscopy Enantioselective Nucleophile Stereochemistry Reduction Cyclization Diastereoselective Alkaloid Catalysis Chiral Auxiliary Enantioselective Reduction Aromatic
Huffman, John W.
Raveendranath, Panolil C.
A completely stereoselective total synthesis of the naturally occuring polyhydroxyagarofuran, (+/-)-isocelorbicol (1) is described.The readily available α-agarofuran derivative 3 was converted to 3β-hydroxy-9-keto-β-agarofuran (6) by epoxidation followed
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