STABLE ROTAMERS ABOUT A SULFUR-TO-CARBON SINGLE BOND IN 1,4-DIMETHOXY-9-BENZYLSULFONYLTRIPTYCENE: THEIR ISOLATION AND CHARACTERIZATION

DOI: 10.1246/cl.1984.143

Source and publish data:

Chemistry Letters p. 143 - 146 (1984)

Update date:2022-08-04

Topics:

Authors:

Nakamura, Nobuo

Oki, Michinori

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Article abstract of DOI:10.1246/cl.1984.143

Oxidation of 1,4-dimethoxy-9-benzylthiotripticene with mCPBA or hydrogen peroxide to the corresponding sulfone and subsequent chromatography on silica gel yielded two stable rotamers about the S-C(9) single bond.Kinetic parameters for their interconversion as well as their spectroscopic data have been also presented.

Full text of DOI:10.1246/cl.1984.143

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