Tetrahedron Letters p. 895 - 898 (1985)
Update date:2022-08-05
Topics:
Uemura, Sakae
Ohe, Kouichi
Fukuzawa, Shin-ichi
Treatment of sec-alkyl phenyl tellurides, except for the cyclohexyl system, with m-chloroperbenzoic acid(MCPBA) in diethyl ether readily afforded the corresponding olefins in good yields presumably via telluroxide elimination together with small amounts of alcohols and ketones.In the pri-alkyl and cyclohexyl cases the adducts between MCPBA and the tellurides were isolated as stable organotellurium(IV) compounds which gave similar elimination products by neat pyrolysis at 220-250 deg C.
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