Journal of Organometallic Chemistry p. 257 - 262 (1985)
Update date:2022-07-30
Topics:
Diel, Bruce N.
The dimer <(CH3)5C5Fe(NO)>2 has been prepared by octane reflux of <(CH3)5C5Fe(CO)2>2 under a NO atmosphere.Oxidative cleavage of the dimer with iodine yields (CH3)5C5Fe(NO)I2.Alkylation with two equivalents of RLi or RMgX (R = CH3, CH2C6H5, or CH2SC6H5) leads to the dialkyl derivatives in good yields.All compounds are new and have been characterized by elemental analyses, IR, mass 1H and 13C NMR spectra.
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Doi:10.1021/jo00225a050
(1985)Doi:10.1021/jo00225a093
(1985)Doi:10.1139/v62-179
(1962)Doi:10.1021/jm00153a002
(1986)Doi:10.1016/0022-328X(85)87385-X
(1985)Doi:10.1039/c9cc07461a
(2019)
