Polyhedron p. 399 - 400 (1988)
Update date:2022-08-28
Topics:
Chisholm, Malcolm H.
Hammond, Charles E.
Huffman, John C.
Addition of LiNMe2 to Mo(NMe2)4 in tetrahydrofuran establishes the equilibrium: Mo(NMe2)4+2LiNMe2THFαMo(NMe2)6Li2. Red crystals of the THF adduct Mo(NMe2)6Li2(THF)2 have been shown to involve an octahedral MoN6 moiety, MoN = 2.12 A (averaged). The lithium atoms cap opposite faces, LiN3MoN3Li, and are ligated by one THF molecule to complete the pseudo tetrahedral coordination of lithium.
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