Bulletin of the Chemical Society of Japan p. 3031 - 3032 (1980)
Update date:2022-08-11
Topics:
Inoue, Yoshihisa
Deguchi, Shokichiro
Hakushi, Tadao
Dehydration of 1,4-, 1,5-, or 1,6- alkanediols over alumina at 220-250 deg C in a distillation apparatus gave the corresponding 5- to 7-membered oxacyclanes in good yield of 51-71percent.Diethylene glycol also gave 1,4-dioxane in 49percent yield, whereas attempted one-step synthesis of crown ethers from polyethylene glycols in a similar manner resulted in the predominant formation of 1,4-dioxane without any trace of crown ether.
View More
Beijing Green Guardee Technology CO,.LTD
Contact:+86-10-69706062
Address:F2 BLdj,5 No.37 Chaoqian Road
Jiangxi Province Bethel Pharmaceutical Co., Ltd.
Contact:+86-795-259 3456 ，+86-15957688008 13566650571
Address:Huangjindui Chemical Park， Shanggao County ，Yichun city，Jiangxi Province
Contact:+86-0311-84455288-844
Address:Mayu Industrial Park, Jinzhou, Hebei, China.
Sinoway International (Jiangsu) Co., Ltd.
Contact:+86-25-86630167
Address:17 Beijing Road (West), Nanjing, China
Contact:86 513 85512619
Address:Rm.1306, Building A, Wenfeng Mansion,168 Gongnong Road, Nantong Jiangsu China
Doi:10.1055/s-0037-1611913
(2019)Doi:10.1134/S1068162020050052
(2020)Doi:10.1016/j.bmc.2008.07.054
(2008)Doi:10.1021/acs.jced.7b00458
(2017)Doi:10.1016/0031-9422(95)00592-U
(1995)Doi:10.1080/00397910902883751
(2009)
