Journal of the Chemical Society. Chemical communications p. 584 - 586 (1990)
Update date:2022-08-30
Topics:
Akaji, Kenichi
Kiso, Yoshiaki
Carpino, Louis A.
The loss of C-terminal dipeptide through diketopiperazine formation during Fmoc-based solid-phase peptide synthesis has been effectively suppressed by anchoring the first Fmoc amino acid chloride to a new 4-(1',1'-dimethyl-1'-hydroxypropyl)phenoxyacetyl handle (DHPP)-resin; this new t-alcohol type DHPP-resin has been successfully applied to the solid-phase synthesis of bradykinin potentiator B (an eleven-residue peptide) (Fmoc = fluoren-9-ylmethoxycarbonyl).
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