Journal of the Chemical Society. Chemical communications p. 647 - 649 (1982)
Update date:2022-08-10
Topics:
Fiandanese, Vito
Marchese, Giuseppe
Naso, Francesco
Ronzini, Ludovico
The room temperature sequential formation of two C-C bonds by reaction of aromatic or aliphatic Grignard reagents with (E)- or (Z)-1-bromo-2-phenylthioethene in the presence of nickel(II) or palladium(II) catalysts provides a novel stereospecific route to a variety of (E)- or (Z)-olefins of the R-CH=CH-R and R1-CH=CH-R2 type, with a stereoselectivity higher than 99percent for the (E) isomers and in the range 95-98percent for the (Z) isomers.
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