High-pressure alkylation of azomethines 1. Synthesis of N-monoalkylanilines

DOI: 10.1007/BF02494657

Source and publish data:

Russian Chemical Bulletin p. 1005 - 1007 (1999)

Update date:2022-08-16

Topics:

Authors:

Agafonov

Dudin Dudin

Preobrazhenskii

Zhulin Zhulin

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Article abstract of DOI:10.1007/BF02494657

Reaction of anils with alkyl halides under high pressure (10 kbar) was studied. Alkylation in polar media (dioxane or acetonitrile) followed by hydrolysis yields pure N-monoalkylanilines in high yields. Optimum conditions for high-pressure alkylation were found.

Full text of DOI:10.1007/BF02494657

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