Bulletin of the Chemical Society of Japan p. 1537 - 1541 (1980)
Update date:2022-08-17
Topics:
Sagae, Hiromitsu
Fujihira, Masamichi
Lund, Henning
Osa, Tetsuo
The oxidation of o-, m-, and p-nitrotoluenes with electro-generated superoxide ion in dimethylformamide was studied using cyclic voltammetry and controlled potential macro-electrolysis.The electrochemical reduction of oxygen in the presence of o- and p-nitrotoluenes yielded the corresponding carboxylic acids because the methyl groups in these derivatives are activated by the nitro group.An intermediate in these oxidations should be the corresponding nitrobenzaldehyde.The reaction mechanism is discussed.
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