Journal of the Chemical Society. Perkin transactions I p. 183 - 190 (1982)
Update date:2022-08-02
Topics:
Pelter, Andrew
Ward, Robert S.
Watson, Derrick J.
Jack, Ibiba R.
A series of isomeric 2,6- and 2,4-diaryl-3,7-dioxabicyclo<3.3.0>octanes have been prepared via the corresponding threo, and erythro-dioxo-diesters.Comparison of their 1H and 13C n.m.r. spectra reveals small differences in chemical shifts and coupling constants which could be diagnostic in assigning structures to such compounds.The structure of 4-hydroxysesamin has been confirmed by direct correlation with sesamin.
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