Carbohydrate Research p. 23 - 28 (1989)
Update date:2022-08-28
Topics:
Irie, Setsuko
Formose reactions initiated by γ-irradiation in the presence of inorganic bases selectively produce ethylene glycol and pentaerythritol as major products at room temperature in the presence of calcium hydroxide.The yield ratio of ethylene glycol to pentaerythritol depends on the initial concentration of formaldehyde.At low concentration, the main product is ethylene glycol, whereas pentaerythritol increases at high concentration.The decomposition of formaldehyde is inhibited by ethanol, a hydroxyl-radical scavenger.These results suggest that radical reactions play an important role in radiation-initiated formose synthesis, in contrast to thermal formose reactions.
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