Tetrahedron Letters p. 835 - 838 (1984)
Update date:2022-08-11
Topics:
Tarhouni, R.
Kirschleger, B.
Rambaud, M.
Villieras, J.
The preparation of monohalomethyllithium XCH2Li is achieved by Bromine-lithium exchange from the corresponding Bromohalomethane in the presence of one equivalent of lithium bromide at -110 degC in THF-Ether-Pentane solutions.This reagent, on coupling with various carbonyl compounds leads to halohydrins, epoxides and α-halomethyl ketones with high yields.
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