Journal of Organic Chemistry p. 4307 - 4310 (1987)
Update date:2022-08-11
Topics:
Purrington, Suzanne T.
Bumgardner, Carl L.
Lazaridis, Nicholas V.
Singh, Phirtu
Treatment of silyl enol ethers of β-diketones with 5percent F2 in N2 results in the formation of 2-fluoro 1,3-diketones.The acyclic derivatives exist as keto tautomers, while the dimedone derivative is enolic.Similarly, the silyl enol ethers of β-keto esters give rise to α-fluoro-β-keto esters.
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