Journal of Fluorine Chemistry p. 475 - 478 (2005)
Update date:2022-08-29
Topics:
Xiao, Ji-Chang
Shreeve, Jean'ne M.
A microwave-assisted fluorination method for 1,3-dicarbonyl compounds using Selectfluor has been developed. 2-Monofluorinated products can be obtained in high yield in neutral reaction conditions with addition of 1 eq. of Selectfluor. Treatment of 1,3-dicarbonyls with 3 eq. of Selectfluor in the presence of tetrabutylammonium hydroxide (TBAH) as the base results in the formation of 2,2-difluorinated derivatives only.
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