faster quenching studies to be performed for commercial
heat treating.
The microstructural evolution in the aluminum alloys could
be easily followed by optical microscopy and TEM. Matrix
precipitation and grain boundary precipitation could be fol-
lowed as a function of cooling rate. Measurements of PFZ
widths followed a linear relationship with the Jominy distance.
The results show that the Jominy end quench test is a power-
ful tool to examine the effects of quench rate and heat treating
parameters. The test is appropriate for many different nonfer-
rous alloys, where the alloy has properties that depend on the
quench rate. It is highly recommended for quenching studies
in age hardened aluminum.
Acknowledgments
Fig. 10 PFZ width as a function of distance from the quenched precip-
itation could be followed as a function of cooling rate. Measurements
of PFZ widths followed a linear relationship with the Jominy distance
The authors thank Century Aluminumy, Ravenswood Facil-
ity, for funding this work.
References
1. W.E. Jominy and A.L. Boegehold: ASM Trans., 1939, vol. 27 (12),
p. 574.
2. “Jominy Test, Standard Method for End-Quench Test for Hardenability
of Steel,” ASTM A255, Annual Book of ASTM Standards, ASTM,
Philadelphia, PA.
was 14 V DC. The disks were then examined in a Philips
EM430 at 300 kV.
Using bright-field conditions, images of four positions at
varying distances from the quenched end were taken (Fig. 9).
At a position close to the quenched end (J ϭ 7 mm), the grains
have a strong diffraction contrast. A mottled appearance is
evident from the presence of strain contrast around the coherent
or semicoherent precipitates. No large precipitates were found
except at the grain boundaries. Evidence of serrated grain
boundaries was found, probably from pinning. At slower cool-
ing rates, larger and coarser precipitates from quenching
occurred at the grain boundaries and at the interior of the grain.
The lack of strain contrast indicates that the precipitates are
now incoherent.
The complete width of the PFZ around the grain boundary
and interior quenching precipitates was measured and plotted
as a function of position from the quenched end (Fig. 10). The
results show that the PFZ increases in size as a linear function
of distance from the quenched end. The results demonstrate
clearly the relationship of the PFZ to cooling rate. In addition,
based on the results of the Jominy end quench, the width of
the PFZ can now be predicted. This has great significance
toward the prediction of properties as a function of heat
treatment.
3. “Methods of Determining Hardenability of Steels,” SAE J406c, Annual
SAE Handbook, SAE, Warrendale, PA.
4. W.E. Jominy: ASM Trans., 1939, vol. 27 (12), p. 1072.
5. V. Hergat: Traitement Thremique, 1981, vol. 153, p. 49.
6. G.T. Brown: in Hardenability Concepts with Applications to Steel,
D.V. Doane and J.S. Kirkaldy, eds., AIME, Warrendale, PA, 1978,
p. 273.
7. A.K. Sheikh: Proc. 3rd Int. Symp. on Advanced Materials, 1993, TMS,
p. 696.
8. J.G. Kura and C.H. Lorig: “Correlation of Cooling Velocity of the
Standard Jominy Hardenability Test with the Cooling Velocity within
the Cross-Section of Plates,” Battelle Memorial Institute Report
S-547, Battelle, Columbus, OH, June 2, 1942.
9. J.G. Kura and C.H. Lorig: “Correlation of Cooling Velocity of the
Standard Jominy Hardenability Test with the Cooling Velocity within
the Cross-Section of Plates,” Battelle Memorial Institute Report
S-547, Columbus, OH, July 23, 1942.
10. T. Toda: J. Jpn. Inst. Met., 1965, vol. 29, p. 237.
11. P.J. Postans: “The Use of Jominy End Quench to Assess the Harden-
ability of Higher Strength Titanium Alloys,” DCAF 070028 Rolls
Royce, Oct. 1, London, U.K., 1983.
12. B.M. Loring, W.H. Baer, and G.M. Carlton: Trans. Am. Inst. Min.,
Met. Eng., 1948, vol. 175, p. 401.
13. W.G.J. ‘tHart, H.J. Kolkman, and L. Schra: “The Jominy End-Quench
Test for the Investigation of Corrosion Properties and Microstructure
of High Strength Aluminum,” NLR Tr 80102U, National Aerospace
Laboratory, NLR, Netherlands, 1980.
14. Conclusions
14. W.G.J. ‘tHart, H.J. Kolkman, and L. Schra: “Effect of Cooling Rate on
Corrosion Properties and Microstructure of High Strength Aluminum
Alloys,” NLR TR 82105 U, National Aerospace Laboratory, NLR,
Netherlands, 1982.
15. D. Hecker: HTM, 1975, vol. 30, p. 268.
16. H. Bomas: HTM, 1975, vol. 30, p. 274.
17. W.E. Arthur, R. Becker, and M.E. Karabin: Proc. Int. Heat Treating
Conf.—Equipment Processing, Rosemont, IL, May 18–20, 1994.
18. R. Becker, M.E. Karabin, and J.C. Liu: Comput. Mater. Modeling -
ASME, 1994, vol. 294, p. 287.
The Jominy end quench has been shown to produce repro-
ducible and expected structures and properties in Ti-6Al-4V,
AAl 7050, and Al 7075. There is no significant effect of radial
heat transfer during the test, making it truly uniaxial heat flow.
Vickers pryamidal hardness yields the best results, in terms of
reproducibility, accuracy, and the ability to resolve differences
over small distances. The cooling rates can be measured and
correlated with cooling rates in various cross sections, allowing
Journal of Materials Engineering and Performance
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