Journal of the Chinese Chemical Society p. 866 - 870 (2021)
Update date:2022-08-11
Topics:
Li, Xiongjian
Huang, Chi
In this study, BiVO4 synthesized by hydrothermal and calcination methods were explored as catalysts in the ammoxidation of dichlorotoluenes to shed light on the structure-reactivity correlations. The BiVO4 samples were characterized by X-ray diffraction (XRD), temperature-programmed reduction (TPR), Brunauer–Emmett–Teller (BET), and UV–Vis spectrophotometry. The results showed that the catalytic activity of BiVO4 greatly relied on the structure variations. The hydrothermal prepared BiVO4 exhibited better catalytic activities as a consequence of its greater structure deformation, with maximum yields of 73.1, 72.2, and 70.8% for 3,4-, 2,4- and 2,6- dichlorobenzonitrles, respectively.
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