Organic Process Research and Development p. 1783 - 1786 (2012)
Update date:2022-08-11
Topics:
Fukui, Yuki
Oda, Shinichi
Suzuki, Hiroyuki
Hakogi, Toshikazu
Yamada, Daisuke
Takagi, Yohei
Aoyama, Yasunori
Kitamura, Hideyuki
Ogawa, Masayoshi
Kikuchi, Junko
A high-yield robust LHMDS-mediated aldol-type reaction of benzyl maltol (2) and benzaldehyde (3) was developed using in situ IR to overcome the problems of low yield and yield fluctuation of the pilot synthesis. In situ IR studies indicated that unexpecte
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