Tetrahedron Letters p. 5583 - 5586 (1994)
Update date:2022-08-22
Topics:
Kumar, Archana
Dittmer, Donald C.
As little as 0.1 molar equivalent of elemental tellurium in combination with excess (up to 3 molar equivalents) reducing agent (HOCH2SO2Na·H2O, NaBH4, or LiEt3BH) effects the telluride-ion mediated transposition of allylic hydroxyl groups and carbon-carbon double bonds that proceeds via the epoxy tosylate. The workup is much more convenient than when a molar equivalent of tellurium is used.
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