Journal of Organometallic Chemistry p. 7 - 11 (1980)
Update date:2022-08-28
Topics:
Watanabe, Hamao
Awano, Ken-Ichi
Ohmori, Manabu
Kodama, Nobuhiro
Sakamoto, Jun-Ichi
et al.
Phenylazotriphenyl- (Ia) and phenylazotrimethyl-silane (Ib) react with alcohols to give the corresponding alkoxytriorganosilane and benzene as the major products.Spectroscopic investigations (UV) suggested that phenyldiazene was formed as an intermediate which afforded the final reaction products.Chemical evidence for the formation of phenyldiazene was obtained by the reaction of Ia with methanol-d in nonane.Phenylazotriorganosilanes are convenient precursors for phenyldiazene.
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