Tetrahedron Letters p. 2189 - 2192 (1991)
Update date:2022-08-16
Topics:
Kraus
Andersh
The reaction of trimer 6 and an alkyl lithium afforded thiolate 7 which reacted with primary halides to produce silyl thioethers in good to excellent yields. The silyl thioethers could be hydrolyzed to the thiols using HF in acetonitrile.
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(1981)