Tetrahedron Letters p. 5625 - 5628 (1990)
Update date:2022-08-04
Topics:
Hashimoto
Saigo
Machida
Hasegawa
2,2-Dimethoxyethyl acrylate, which is easily prepared by the Mitsunobu reaction, reacts with dienes at -78°C in the presence of a Lewis acid such as titanium(IV) chloride to afford the corresponding Diels-Alder adducts in high yields.
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