Bulletin of the Chemical Society of Japan p. 1188 - 1190 (1982)
Update date:2022-07-29
Topics:
Saigo, Kazuhiko
Miura, Hisao
Ishizaki, Kozi
Nohira, Hiroyuki
(+/-)-2-Amino-2-phenylethanol (phenylglycinol) prepared from (+/-)-2-amino-2-phenylacetic acid (DL-phenylglycine) by lithium aluminium hydride reduction was efficiently resolved into a pair of optically active forms by preferential crystallization.The optically active amino alcohol was successfully applied as a basic resolving agent to the resolution of tartaric acid, 2-hydroxy-2-phenylpropionic acid, 2-hydroxy-3-phenylpropionic acid, 2-phenylpropionic acid, and 2-phenyl-2-ureidoacetic acid.
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