Tetrahedron Letters p. 355 - 356 (1996)
Update date:2022-08-10
Topics:
Berkessel, Albrecht
Geisel, Urs
Herault, David A.
cyclo-2,3-Diphospho-D-glycerate (c-DPG) was synthesized from D-mannitol in seven steps on a gram-scale. Key feature of the synthetic route is the cyclization of methyl 2,3-diphospho-D-glycerate using dicyclohexylcarbodiimide. The preparation described makes the natural product c-DPG available on a larger scale for the first time.
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