
Tetrahedron p. 1301 - 1310 (1997)
Update date:2022-08-17
Topics:
Junggebauer, Joerg
Neumann, Wilhelm P.
A polymer-supported distannane 1 was prepared by treatment of tin halide resin with lithium naphthalenide or sodium naphthalenide in THF. The content of the polymers 1 was determined to be 0.95 to 1.13 mmol/g tin as ditin. The polymer-supported distannane reagent was successfully applied to radical cyclizations of acyclic α-haloesters to yield γ-butyrolactones.
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(1955)