Journal of labelled compounds and radiopharmaceuticals p. 47 - 51 (1998)
Update date:2022-08-31
Topics:
Chauviere
Rousseau
Pillon
Perie
2-Amino-5-(1-methyl-5-nitro-4-iodo-2-imidazoyl)-1,3,4-thiadiazole (5) was prepared from imidazole via a 4-steps sequence. Reductive desiodination of 5 using a tetrahydrofuran solution of NaBH4 in the presence of tritiated water provided the title compound (specific radioactivity 12.6 Ci/mmol) in one step.
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