Tetrahedron Letters p. 7307 - 7308 (1998)
Update date:2022-08-25
Topics:
Nishikawa, Asuka
Hashimoto, Yuichi
Shirai, Ryuichi
The Lewis acid-promoted reaction of 3-butyl-7-methoxyphthalide with butanethiol gave the thiophthalide, which was converted to 6-amylsalicylic acid by alkaline hydrolysis and successive desulfurization by Raney Ni.
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