Tetrahedron p. 809 - 829 (1991)
Update date:2022-08-10
Topics:
Coleman
Hallcher
HcMackins
Rogers
Wagenknecht
An efficient, practical, electrochemical system was developed for the synthesis of a mixture of 4-acetoxy-5-hexenoic acid and trans-6-acetoxy-4-hexenoic acid via manganese (III)-mediated oxidation of acetic acid-acetic anhydride in the presence of butadiene. Copper (II) co-catalyst enhanced the efficiency of this oxidation and copper (I) was shown to catalyze in situ conversion of the acetoxyhexenoic acids into γ-vinyl-γ- butyrolactone.
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