Synthesis and reactions of 4-tributylstannyl-3-methylisoxazole

DOI: 10.3987/com-96-7489

Source and publish data:

Heterocycles p. 1301 - 1304 (1996)

Update date:2022-08-17

Topics:

Authors:

Uchiyama, Daishi

Yabe, Makoto

Kameyama, Hiroshi

Sakamoto, Takao

Kondo, Yoshinori

Yamanaka, Hiroshi

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Article abstract of DOI:10.3987/com-96-7489

1,3-Dipolar cycloaddition reaction of bis(tributylstannyl)acetylene with nitrile oxides, followed by treatment with aqueous ammonia in ethanol in a sealed tube gave 4-tributylstannyl-3-methylisoxazole. The palladium catalyzed cross coupling reaction of the isoxazole with 2-iodonitrobenzene, followed by reductive cyclization afforded 3-acetylindole.

Full text of DOI:10.3987/com-96-7489

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Product name:Isoxazole, 3-methyl-4-phenyl- (7CI,8CI,9CI)

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