Journal of the Chemical Society. Perkin transactions II p. 773 - 776 (1983)
Update date:2022-08-17
Topics:
Bonningue, Corine
Houalla, Douraid
Wolf, Robert
Jaud, Joel
The dimerization of 3,3,7,7-tetramethyl-2,8-dioxa-5-aza-1-phosphaIIIbicyclo<3.3.0>octane (1) leads to octahydro-2,2,6,6,10,10,14,14-octamehylbis-1,2,3-oxazaphospholo<2,3-b:2',3'-g>-1,6,3,8,2,7-dioxadiazadiphosphecine (2), a tricyclic compound with sixteen atoms around the periphery.The preparation, identification, and the X-ray structure are described.A pathway for the formation of the dimer is suggested by the trans-position of the two phosphorus ione pairs.
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