Chemistry Letters p. 249 - 250 (1995)
Update date:2022-08-11
Topics:
Maeda, Hatsuo
Maki, Toshihide
Ohmori, Hidenobu
The species generated by one-electron transfer to acyl tributylphosphonium ions has proved to be potent acyl radical equivalents by the results that unsubstituted and 6-phenyl- substituted 5-hexenoic acids were transformed into cyclopentanones by the electrolysis in the presence of Bu3P in an undivided cell, although the yields were not satisfactory due to the formation of 5-hexen-1-als via further one-electron reduction of the radicals before their cyclization.
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