Tetrahedron Letters p. 4397 - 4400 (1991)
Update date:2022-08-11
Topics:
Herdewijn
Kerremans
Wigerinck
Vandendriessche
Van Aerschot
A simple, high yield synthesis of thymidine from 5-iodo-2'-deoxyuridine is described, using tetramethyltin and tetrakis(triphenylphosphine)palladium(0) in hexamethylphosphoric triamide. Likewise, 5-phenyl- and 5-vinyl-2'-deoxyuridine can be obtained, and through reduction of the latter the 5-ethyl analogue is also at hand.
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