Stereoselective syntheses of 1,24-dihydroxy squalene 2,3;22,23-dioxides by double Sharpless epoxidation

DOI: 10.1016/S0040-4039(96)02332-5

Source and publish data:

Tetrahedron Letters p. 383 - 386 (1997)

Update date:2022-08-11

Topics:

Authors:

Hauptfleisch, Roland

Franck, Burchard

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Article abstract of DOI:10.1016/S0040-4039(96)02332-5

A few step synthesis of the (all-E) squalene diol 10 from squalene 4, its double Sharpless epoxidation to the (-)-dihydroxy squalene 2,3;22,23-dioxide 3a, its enantiomer 3b, and the formation of a tetradeutero derivative 12 is described.

Full text of DOI:10.1016/S0040-4039(96)02332-5

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