Journal of Organic Chemistry p. 4968 - 4970 (1982)
Update date:2022-08-16
Topics:
Campbell, Jo-Anne B
Deinzer, Max L.
Miller, Terry L.
Rohrer, Douglas C.
Strong, Phyllis, E.
Reduction of 2,3,4,5,6-pentachloro-4-(pentachlorophenoxy)-2,5-cyclohexadienone (3) yields nonachloro-4-phenoxyphenol (2) and nonachloro-2-phenoxyphenol (4) in varying amounts, depending on the nature of the reaction scheme.Mechanistic pathways for the formation of 2 and 4 from 3 are suggested.The structure of 3 was confirmed by X-ray crystallography.The carbon-13 NMR spectrum of 2 is described.
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