Journal of Fluorine Chemistry p. 17 - 28 (1990)
Update date:2022-08-11
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Eapen, K. C.
The zinc coupling reaction of a pure sample of 2,2-Dichlorotrifluoro-1-iodoethane (I) in acetic anhydride-methylene chloride has been investigated.The coupled product C4F6Cl4 was found to be a single isomer by 19F NMR and had the structure CFCl2CF2CF2CFCl2 (II).The probable modes of formation of by-products such as C6F9Cl5 and C8F12Cl6 are discussed.
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