A secure and convenient synthesis of 5-amino-1, 2, 3-thiadiazole by diazoacetonitrile

DOI: 10.3987/COM-96-7399

Source and publish data:

Heterocycles p. 197 - 201 (1997)

Update date:2022-08-16

Topics:

Authors:

Harada, Katsumasa

Mori, Yoshikatsu

Nakai, Mamoru

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Article abstract of DOI:10.3987/COM-96-7399

A new synthesis of 5-amino-1,2,3-thiadiazole (3) by diazoacetonitrile (2) and H₂S in the presence of a base is described. The compound (2) is undoubtedly explosive but with our method we found it could be used for industrial purposes.

Full text of DOI:10.3987/COM-96-7399

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