Research on Chemical Intermediates p. 645 - 649 (2012)
Update date:2022-08-29
Topics:
Chen, Xinzhi
Li, Guihua
Qian, Chao
Oxidization of O,O,O-trimethyl phosphorothioate to the corresponding oxo (P=O) compound is accomplished under mild conditions with hydrogen peroxide or ozone. Urea hydroperoxide was found to be a serviceable solid-state source of hydrogen peroxide; it was a better oxidizing agent than 30% hydrogen peroxide and resulted in better yield. It was also proved that ozone was the most effective oxidizer, with formation of purer products in higher yield (90.1%) than with hydrogen peroxide. Springer Science+Business Media B.V. 2011.
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