Journal of the Chemical Society. Perkin transactions I p. 3135 - 3140 (1981)
Update date:2022-08-17
Topics:
Bonnett, Raymond
Ridge, Richard J.
Scourides, Panayiotis A.
Berenbaum, Morris C.
The components of haematoporphyrin derivative ( a preparation used as a photosensitiser in clinical applications, and made by treating haematoporphyrin with sulphuric acid-acetic acid) have been separated by preparative h.p.l.c. and identified by comparison with authentic porphyrincarboxylic acids.The composition of the mixture is somewhat variable but the main components are O,O'-diacetylhaematoporphyrin (6) and O-acetylhaematoporphyrin (2)/(3) with smaller amounts of the 8(3)-(1-acetoxyethyl)-3(8)-vinyldeuteroporphyrin isomers (7) and (8) and the corresponding alcohols (4) and (5).
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