Journal of Fluorine Chemistry p. 235 - 240 (1985)
Update date:2022-08-24
Topics:
Unemoto, Teruo
Gotoh, Yoshihiko
(1,1-Dihydroperfluoroalkyl)phenyl- and -p-fluorophenyliodonium triflates 2 and 3 were synthesized by the reaction of 1-bis(trifluoroacetoxy)iodo-1,1-dihydroperfluoroalkanes 1 with triflic acid and benzene or fluorobenzene in 1,1,2-trichloro-trifluoroethane.The use of fluorosulfonic acid and sulfuric acid instead of triflic acid afforded (1,1-dihydroperfluoroalkyl)phenyliodonium fluorosulfonate 4 and sulfate 5, respectively.Similarly, (1,1,ω-trihydroperfluoroalkyl)phenyliodonium triflate 7 and 1,1,5,5-tetrahydroperfluoropentane-1,5-bisphenyliodonium triflate 9 were synthesized.
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