Resin glycosides. XVIII. Determination by Mosher's method of the absolute configurations of mono- and dihydroxyfatty acids originated from resin glycosides

DOI: 10.1248/cpb.41.1023

Source and publish data:

Chemical and Pharmaceutical Bulletin p. 1023 - 1026 (1993)

Update date:2022-08-10

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Authors:

Ono Ono

Yamada Yamada

Noda Noda

Kawasaki

Miyahara

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Article abstract of DOI:10.1248/cpb.41.1023

The absolute configurations of four hydroxyfatty acids, jalapinolic acid, convolvulinolic acid, ipurolic acid and 3,11-dihydroxyhexadecanoic acid, obtained by acid hydrolysis of various resin glycosides, have been determined to be 11S,11S,3S,11S, and 3S,11S, respectively, by Mosher's method. The R- configuration of jalapinolic acid previously defined by Horeau's method was therefore revised to S.

Full text of DOI:10.1248/cpb.41.1023

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