Synthesis p. 1195 - 1198 (1997)
Update date:2022-08-17
Topics:
Reyes, Elba D.
Carballeira, Nestor M.
The antimicrobial marine fatty acid (5Z,9Z)-14-methylpentadeca-5,9-dienoic acid, recently identified in the phospholipids of the Caribbean gorgonian Eunicea succinea, and its longer-chain analog (5Z,9Z)-24-methylpentacosa-5,9-dienoic acid, initially identified in the phospholipids of the sponge Petrosia ficiformis, have been synthesized for the first time through a common synthetic route. A combination of alkyne-bromide coupling and Wittig reaction resulted in the best combination for assembling the Δ5,9 functionality in high yield and stereoselectivity.
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(1980)
