Synthetic Communications p. 149 - 155 (1995)
Update date:2022-08-03
Topics:
Mincheva
Velkov
Boireau
Barry
Fugier
2'-Hydroxy-6'-methoxyacetophenone was obtained in 66% yield from 3-methoxyphenol. In the key step, 3-methoxyphenol protected by means of ethylvinyl ether was selectively metallated at the 2-position with butyllithium. Addition of ZnCl2 to the aryllithium gave the corresponding organozinc compound, which readily reacted on acetyl chloride under palladium catalysis.
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