Determination of enantiomeric purity of hydroxy biaryls using1H and31P-NMR on their diazaphospholidine derivatives

DOI: 10.1016/S0040-4039(00)77044-4

Source and publish data:

Tetrahedron Letters p. 5125 - 5128 (1994)

Update date:2022-08-11

Topics:

Authors:

Alexakis

Frutos Frutos

Mangeney

Meyers Meyers

Moorlag, Henk

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Article abstract of DOI:10.1016/S0040-4039(00)77044-4

Chiral biaryl alcohols were readily transformed in a single step, with chiral non-racemic 1,2-diamines, PCl₃, and sulfur in CDCl₃ - all in a NMR tube - to their diastereomeric diazaphospholidines and their diastereomeric ratios (also

Full text of DOI:10.1016/S0040-4039(00)77044-4

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