Solid State Communications p. 813 - 816 (1987)
Update date:2022-08-11
Topics:
Greneche, J. M.
Varret, F.
Leblanc, M.
Ferey, G.
Isothermal and non-isothermal treatments were performed on amorphous fluorides vapor-deposited FeF//2 and FeF//3, xHF (0. 4 less than x less than 1. 0) obtained by a soft chemistry reaction. They crystallize in rhombohedral and/or hexagonal tungsten bronze type phases, evidenced by Mossbauer spectroscopy and X-ray diffraction. The influence of the experimental parameters is discussed: heating modes and pressure. It is concluded that the 'ideal' amorphous FeF//3 crystallizes in the rhombohedral form.
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