Darstellung and Characterisierung der kationischen Metallocen-Komplexe 2 und : Laborsynthese von UF6

DOI: 10.1016/0022-328X(93)83279-5

Source and publish data:

Journal of Organometallic Chemistry p. 91 - 94 (1993)

Update date:2022-08-30

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Authors:

Schulz, Axel

Klapoetke, Thomas M.

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Article abstract of DOI:10.1016/0022-328X(93)83279-5

The five-coordinate, dicationic complex 2 (1) was formed by reaction of Cp2ZrCl2 and 2 equiv. of AgAsF6 in acetonitrile.A stable, polymeric niobocenium UF6 complex, (2), was synthesized from Cp2NbCl2 and UF6.A convenient laboraotry-scale synthesis of pure UF6 is reported.

Full text of DOI:10.1016/0022-328X(93)83279-5

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