Tetrahedron Letters p. 1933 - 1936 (1984)
Update date:2022-08-16
Topics:
Murata, Shigeru
Sugawara, Tadashi
Nakashima, Nobuaki
Yoshihara, Keitaro
Iwamura, Hiizu
Laser-flash photolysis studies have been carried out on a solution of ap- and sp-9-(2-azido-4,6-dimethylphenyl)fluorenes (3) in methanol-ether at 25 deg C.The rates of formation of azanorcaradiene (5) from ap-nitrene (4)ap, and of 9-methoxyfluorene (7) from o-quinoid intermediate (6) were determined.The deuterium isotope effect on the migration of the hydrogen is discussed.
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