Archiv der Pharmazie p. 912 - 915 (1983)
Update date:2022-08-17
Topics:
Knabe
Lorenz
The title compound 4 is synthesized from the 7-chlorotheinopyridine 1 via the 7-(dimethoxybenzyl) compound 2 which is obtained by Wittig alkylation. Compound 2 is methylated by methyl iodide to give the iminium salt 3 which is reduced with LiAlH4 to yield 4. When 4 is treated with 0.1 N-HCl the disproportionation products 3 and 5 are formed. Moreover, the rearrangement product 6 is obtained in 6% yield. Compound 6 was isolated as the pseudocyanide 7.
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Doi:10.1016/0040-4039(94)88184-7
(1994)Doi:10.1016/S0040-4039(00)90586-0
(1967)Doi:10.1016/j.foodchem.2015.04.079
(2015)Doi:10.1016/j.jsbmb.2019.02.006
(2019)Doi:10.3762/bjoc.14.211
(2018)Doi:10.1080/24701556.2018.1503677
(2018)
